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Proceedings of Singapore Conference

www.econferenceglobe.com 
13
Uzbekistan by officials of ministries, state committees and departments - from seven-fold 
base amount (1,561,000 soums) up to ten times (2,230,000 soums). , in case of repeated - from 
ten times the base amount of the calculation (1,561,000 soums) to fifteen times (3,345,000 
soums) shall result in the imposition of a fine in the amount of rupees. 
In connection with the above, the Code of Administrative Responsibility also provides 
for the establishment of responsibility for providing texts of regulatory legal acts and 
protecting the rights and interests of individuals and legal entities: 
unofficial publication of normative legal acts subject to official publication
implementation of a normative legal act, which should be officially published, but not 
officially published. 
Conclusion 
In conclusion, these types of responsibility can be expressed in the article itself or in a 
separate article, with a logical continuation of article 198[3]. 
References 
1. The Constitution of the Republic of Uzbekistan. 
2. Law of the Republic of Uzbekistan "On regulatory legal acts". 
3. Code of administrative responsibility. 


5th Global Congress on Contemporary Sciences & Advancements 
Hosted from Singapore 
10th May 2021 
www.econferenceglobe.com 
14
OBTAINING OF PURIFIED CARBOXYMETHYL CELLULOSE 
SODIUM BY USING MINERAL ACIDS 
Goyibnazarov Ilkhom Shukhrat ogli
Institute of polymer chemistry and physics of Uzbekistan Academy of Sciences
E-mail:igoyibnazarov@bk.ru 
Karabaeva Barno Sabirovna
Institute of polymer chemistry and physics of Uzbekistan Academy of Sciences 
Nazarova Zilola Madjitovna
Institute of polymer chemistry and physics of Uzbekistan Academy of Sciences 
Nishanova Saodat Ravshan kizi 
Institute of polymer chemistry and physics of Uzbekistan Academy of Sciences 
Yuldoshov Sherzod Abdullaevich,
Institute of polymer chemistry and physics of Uzbekistan Academy of Sciences, PhD, senoir 
researcher. 
E-mail:
sherzodbek)y@mail.ru 
Sarimsokov Abdushkur Abdukhalilovich,
Institute of polymer chemistry and physics of Uzbekistan Academy of Sciences, Professor. E-
mail: 
sarimsakov1948@mail.ru
 
Abstract: This article describes the conditions and advantages of purifying technical Na-CMC 
using sulfuric acid. In the sulfuric acid purification method, technical Na-CMC is converted to 
a water-insoluble H-CMC form and the concentration is achieved by washing in water to 
remove an organic and inorganic salts mixture. H-CMC, which is insoluble in purified water, 
is converted to Na-CMC water-soluble form using an alcoholic sodium hydroxide solution. By 
using this method, it was possible to obtain a high-purity product and reduce energy and 
material consumption.
Keywords: Carboxymethylcellulose, purification, mineral acids, IR spectroscopy, sulfuric acid 
method 
Introduction
Purified Na-CMC producing countries are mainly France, Germany, China, Finland, 
the Netherlands and Mexico. These countries are supply purified Na-CMC to other countries 
[1].
It is known that the technical Na-CMC purity level is not produced on the basis of 
special requirements, therefore, depending on the application, it is important to remove heavy 
metal salts from its composition [2]. 
Na-CMC, which has a high purity degree, is used for pharmaceuticals and food. Na-
CMC mineral acids with high purity are used [3]. 
The effect of different mineral acids on the technical Na-CMC purification process was 
studied, and it was found that the effect of the acids was different. Therefore, different 
concentrations solutions of acids were used in the cleaning process. The most influenceive 
purification method with mineral acids was found to be the sulfuric acid method. Technical 
Na-CMC was reacted with 20% sulfuric acid in a 1:10 modulus ratio for 2 hours.The H-CMC 
obtained in the reaction was removed from the additional salts by washing in water. The 
purified H-CMC reaction with sodium hydroxide was carried out for 2 hours to obtain a 
completely soluble product Na-CMC. The fully purified H-CMC was converted to a water-


5th Global Congress on Contemporary Sciences & Advancements 
Hosted from Singapore 
10th May 2021 

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